How to Prepare Tungsten Diselenide?

Tungsten diselenide WSe2 can be obtained by reacting tungsten and stoichiometric selenium powder in a vacuum-sealed quartz tube at 600-700°C.

Heating the tungsten flake in a high-pressure and high-temperature (over 800 K) selenium vapor, using sputtering deposition technology can form hexagonal crystals with the correct element ratio on the flake:

W+2Se→WSe2

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